6F4J
Crystal structure of Drosophila melanogaster SNF/U2A' complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | BESSY BEAMLINE 14.1 |
| Synchrotron site | BESSY |
| Beamline | 14.1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2014-09-18 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 0.9184 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 65.978, 53.763, 75.839 |
| Unit cell angles | 90.00, 103.09, 90.00 |
Refinement procedure
| Resolution | 19.905 - 1.420 |
| R-factor | 0.1482 |
| Rwork | 0.146 |
| R-free | 0.19320 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.183 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.500 |
| High resolution limit [Å] | 1.420 | 1.420 |
| Number of reflections | 97210 | |
| <I/σ(I)> | 10.3 | |
| Completeness [%] | 99.0 | |
| Redundancy | 3.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | BATCH MODE | 277 | 0.2 M Li2SO4, 0.1 M sodium cacodylate, pH 6.5, 30 % (w/v) PEG 400 |
