6F4G
'Crystal structure of the Drosophila melanogaster SNF/U2A'/U2-SL4 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-07-03 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.9184 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 65.045, 103.914, 116.350 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.442 - 1.900 |
R-factor | 0.1687 |
Rwork | 0.167 |
R-free | 0.21770 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.015 |
RMSD bond angle | 1.398 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.010 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.140 | |
Number of reflections | 62952 | |
<I/σ(I)> | 11.64 | |
Completeness [%] | 99.7 | |
Redundancy | 5.78 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH MODE | 277 | 20 % (w/v) PEG 3350, 0.2 M Li2SO4 and 15 mM sarcosine as an additive |