6F3Y
Backbone structure of Des-Arg10-Kallidin (DAKD) peptide bound to human Bradykinin 1 Receptor (B1R) determined by DNP-enhanced MAS SSNMR
Spectrometer
Experimental method: SOLID-STATE NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | AVANCE II | 400 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 2D 13C-13C DQ-SQ |
| 10 | 1 | 5 | 2D 15N-13C TEDOR |
| 11 | 1 | 6 | 2D 13C-13C DQ-SQ |
| 12 | 1 | 6 | 1D REDOR/DQF double-filter 13C |
| 13 | 1 | 6 | 2D 13C-13C DQ-SQ |
| 2 | 1 | 1 | 2D 15N-13C TEDOR |
| 3 | 1 | 2 | 2D 13C-13C DQ-SQ |
| 4 | 1 | 2 | 2D 15N-13C TEDOR |
| 5 | 1 | 3 | 2D 13C-13C DQ-SQ |
| 6 | 1 | 5 | 2D 13C-13C DQ-SQ |
| 7 | 1 | 4 | 2D 15N-13C TEDOR |
| 8 | 1 | 4 | 2D 13C-13C DQ-SQ |
| 9 | 1 | 3 | 2D 15N-13C TEDOR |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 7.6 | 1 | 110 |
Conformers
| Conformers Calculated Total Number | 500 |
| Conformers Submitted Total Number | 10 |
