6F0T
Crystal structure of Pizza6-SFW
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-12-16 |
| Detector | DECTRIS PILATUS 6M-F |
| Wavelength(s) | 0.9795 |
| Spacegroup name | P 1 |
| Unit cell lengths | 32.529, 69.454, 78.710 |
| Unit cell angles | 65.36, 89.80, 77.16 |
Refinement procedure
| Resolution | 38.930 - 1.740 |
| R-factor | 0.1945 |
| Rwork | 0.192 |
| R-free | 0.23330 |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.842 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 38.930 | 1.770 |
| High resolution limit [Å] | 1.740 | 1.740 |
| Rmerge | 0.053 | 0.635 |
| Rpim | 0.043 | 0.499 |
| Number of reflections | 61581 | |
| <I/σ(I)> | 11.4 | |
| Completeness [%] | 98.5 | 96.1 |
| Redundancy | 4.1 | 4.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 291.15 | 0.25 M calcium chloride 15% (w/v) PEG6000, and 0.1 M MES pH 6.0 |
