6F0G
Crystal structure ASF1-ip3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 80 |
Detector technology | CCD |
Collection date | 2011-03-08 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.98011 |
Spacegroup name | H 3 2 |
Unit cell lengths | 73.470, 73.470, 343.860 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 38.880 - 2.300 |
R-factor | 0.2129 |
Rwork | 0.210 |
R-free | 0.26730 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.160 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | BUSTER |
Refinement software | BUSTER (2.8.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.000 | 2.440 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.025 | 0.130 |
Number of reflections | 16434 | |
<I/σ(I)> | 8.3 | |
Completeness [%] | 99.6 | 97.5 |
Redundancy | 7.9 | 7.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | Citrate 0.1M pH 2.5, LiSO4 0.25M, PEG8000 7% |