6EXZ
Crystal structure of Mex67 C-term
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-01-21 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.97949 |
Spacegroup name | P 61 |
Unit cell lengths | 71.419, 71.419, 20.343 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.925 - 1.300 |
R-factor | 0.1714 |
Rwork | 0.170 |
R-free | 0.20670 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1oai |
RMSD bond length | 0.009 |
RMSD bond angle | 1.203 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.930 | 1.350 |
High resolution limit [Å] | 1.300 | 1.300 |
Rmerge | 0.045 | |
Rmeas | 0.046 | |
Number of reflections | 14960 | |
<I/σ(I)> | 28.54 | |
Completeness [%] | 100.0 | 100 |
Redundancy | 19 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 294 | 35% Tacsimate pH 7 |