6EVH
Lipoaminopeptide helioferin A and B from Mycogone rosea
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SEALED TUBE |
Source details | BRUKER IMUS MICROFOCUS |
Temperature [K] | 100 |
Detector technology | CMOS |
Collection date | 2017-06-07 |
Detector | RDI CMOS_8M |
Wavelength(s) | 1.54178 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 34.711, 10.886, 17.150 |
Unit cell angles | 90.00, 93.05, 90.00 |
Refinement procedure
Resolution | 17.300 - 0.900 |
R-factor | 0.0856 |
Rwork | 0.085 |
R-free | 0.09320 |
Structure solution method | AB INITIO PHASING |
Data reduction software | PROTEUM PLUS |
Data scaling software | SAINT |
Phasing software | SHELXS |
Refinement software | SHELXL |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 17.300 | 1.000 |
High resolution limit [Å] | 0.820 | 0.900 |
Number of reflections | 11314 | |
<I/σ(I)> | 26.2 | |
Completeness [%] | 91.5 | |
Redundancy | 9.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 297 | slow evaporation in a closed vial |