6EVH
Lipoaminopeptide helioferin A and B from Mycogone rosea
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SEALED TUBE |
| Source details | BRUKER IMUS MICROFOCUS |
| Temperature [K] | 100 |
| Detector technology | CMOS |
| Collection date | 2017-06-07 |
| Detector | RDI CMOS_8M |
| Wavelength(s) | 1.54178 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 34.711, 10.886, 17.150 |
| Unit cell angles | 90.00, 93.05, 90.00 |
Refinement procedure
| Resolution | 17.300 - 0.900 |
| R-factor | 0.0856 |
| Rwork | 0.085 |
| R-free | 0.09320 |
| Structure solution method | AB INITIO PHASING |
| Data reduction software | PROTEUM PLUS |
| Data scaling software | SAINT |
| Phasing software | SHELXS |
| Refinement software | SHELXL |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 17.300 | 1.000 |
| High resolution limit [Å] | 0.820 | 0.900 |
| Number of reflections | 11314 | |
| <I/σ(I)> | 26.2 | |
| Completeness [%] | 91.5 | |
| Redundancy | 9.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | EVAPORATION | 297 | slow evaporation in a closed vial |
