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6EV5

Crystal structure of E282Q A. niger Fdc1 with prFMN in the hydroxylated form

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I03
Synchrotron siteDiamond
BeamlineI03
Temperature [K]100
Detector technologyPIXEL
Collection date2017-07-22
DetectorDECTRIS PILATUS3 S 6M
Wavelength(s)0.976
Spacegroup nameP 21 21 2
Unit cell lengths96.020, 63.510, 87.620
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution38.300 - 1.280
R-factor0.16711
Rwork0.166
R-free0.19027
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4za4
RMSD bond length0.024
RMSD bond angle2.375
Data reduction softwarexia2
Data scaling softwarexia2
Phasing softwareREFMAC
Refinement softwareREFMAC (5.8.0158)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]38.3001.326
High resolution limit [Å]1.2801.280
Rmeas1.535
Number of reflections13339713301
<I/σ(I)>8.81
Completeness [%]96.0
Redundancy4.54.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP2770.2 M potassium thiocyanate, Bis-Tris propane pH 6.5, 20% w/v PEG 3350

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