6EU4
Structure of Acinetobacter phage vb_AbaP_AS12 gp42 tailspike
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-10-21 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.978820 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 93.202, 143.336, 176.515 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.771 - 1.794 |
R-factor | 0.1263 |
Rwork | 0.125 |
R-free | 0.14560 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 0.900 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | SHELXDE |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.900 |
High resolution limit [Å] | 1.790 | 1.790 |
Rmeas | 0.088 | 0.378 |
Number of reflections | 425170 | 66612 |
<I/σ(I)> | 16 | 4.71 |
Completeness [%] | 99.4 | 96.3 |
Redundancy | 6.94 | 6.75 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | PEG 6,000, malic acid |