6EST
INTERACTION OF THE PEPTIDE CF3-LEU-ALA-NH-C6H4-CF3(TFLA) WITH PORCINE PANCREATIC ELASTASE. X-RAY STUDIES AT 1.8 ANGSTROMS
Experimental procedure
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 51.480, 57.980, 75.140 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | ? - 1.800 |
| Rwork | 0.200 |
| RMSD bond length | 0.020 |
| RMSD bond angle | 2.500 |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | |
| Rmerge | 0.092 * |
| Number of reflections | 11526 * |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, sitting drop * | 5.7 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | PPE | ||
| 2 | 1 | 1 | acetate | ||
| 3 | 1 | 1 | TFLA | 10:1 excess | |
| 4 | 1 | 1 | DME | ||
| 5 | 1 | 1 | ammonium sulfate |
