6EP6
ARABIDOPSIS THALIANA GSTU23, reduced
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-05-17 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9686 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 88.597, 50.449, 113.702 |
Unit cell angles | 90.00, 108.66, 90.00 |
Refinement procedure
Resolution | 44.179 - 1.592 |
R-factor | 0.1904 |
Rwork | 0.189 |
R-free | 0.21980 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vo4 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.002 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.690 |
High resolution limit [Å] | 1.590 | 1.590 |
Rmerge | 0.100 | 1.390 |
Number of reflections | 64020 | |
<I/σ(I)> | 16.16 | 3.02 |
Completeness [%] | 97.6 | 92.9 |
Redundancy | 6.4 | 6.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 273 | 0.16 M MGCL2, 0.08 M TRIS PH 8.5, 24% PEG4000, 20% GLYCEROL |