6ENV
X-ray structure of Au2phen-encapsulated horse spleen apoferritin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-09-14 |
Detector | RIGAKU SATURN 944 |
Wavelength(s) | 1.5418 |
Spacegroup name | F 4 3 2 |
Unit cell lengths | 180.967, 180.967, 180.967 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 104.480 - 1.820 |
R-factor | 0.147 |
Rwork | 0.145 |
R-free | 0.17500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5erk |
RMSD bond length | 0.022 |
RMSD bond angle | 1.952 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 104.500 | 1.850 |
High resolution limit [Å] | 1.820 | 1.820 |
Rmerge | 0.121 | 0.690 |
Rpim | 0.126 | 0.269 |
Number of reflections | 23324 | |
<I/σ(I)> | 11.9 | |
Completeness [%] | 99.9 | |
Redundancy | 12.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 0.6-0.8 M (NH4)2SO4, 0.1 M Tris pH 7.4-7.7, 50-60 mM CdSO4 |