6ELX
Oryza sativa DWARF14
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-2 |
| Synchrotron site | ESRF |
| Beamline | ID23-2 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2012-11-21 |
| Detector | DECTRIS PILATUS3 X 2M |
| Wavelength(s) | 0.99188 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 48.120, 88.640, 118.940 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 44.610 - 1.350 |
| R-factor | 0.161 |
| Rwork | 0.159 |
| R-free | 0.17700 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1wom |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.785 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((DEV_2880: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.610 | 1.400 |
| High resolution limit [Å] | 1.350 | 1.350 |
| Rmerge | 0.051 | 0.418 |
| Number of reflections | 107538 | |
| <I/σ(I)> | 16.15 | |
| Completeness [%] | 95.7 | 77.3 |
| Redundancy | 4.8 | 4.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | HEPES pH 7.0, 2-methylpentandiol |
