6ELQ
Carbon Monoxide Dehydrogenase IV from Carboxydothermus hydrogenoformans
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-06-22 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.91841 |
Spacegroup name | P 3 2 1 |
Unit cell lengths | 209.150, 209.150, 93.410 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 45.626 - 2.520 |
R-factor | 0.2362 |
Rwork | 0.235 |
R-free | 0.27470 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.534 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1-2575_1168: ???)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 46.700 |
High resolution limit [Å] | 2.520 |
Number of reflections | 79240 |
<I/σ(I)> | 10.5 |
Completeness [%] | 100.0 |
Redundancy | 15.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 20 % (v/v) Polypropoylene glycol 400, 10 % (v/v) 1-Propanol |