6EEQ
Crystal structure of Rhodiola rosea 4-hydroxyphenylacetaldehyde synthase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2017-12-03 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.979100 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 118.360, 118.360, 67.040 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 83.693 - 2.600 |
R-factor | 0.216565229469 |
Rwork | 0.211 |
R-free | 0.26852 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.751 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 118.420 | 2.490 |
High resolution limit [Å] | 2.400 | 2.400 |
Number of reflections | 18852 | |
<I/σ(I)> | 23.8 | |
Completeness [%] | 97.8 | |
Redundancy | 23.8 | |
CC(1/2) | 0.999 | 0.486 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 0.21M potassium thiocyanate and 22% w/v PEG 3350 |