6EEL
Crystal Structure of Myoferlin C2A with divalent cation
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL7-1 |
Synchrotron site | SSRL |
Beamline | BL7-1 |
Temperature [K] | 90 |
Detector technology | CCD |
Collection date | 2015-02-08 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.1271 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 47.350, 83.110, 94.280 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 62.340 - 1.930 |
R-factor | 0.1857 |
Rwork | 0.181 |
R-free | 0.23200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2dmh |
RMSD bond length | 0.017 |
RMSD bond angle | 1.853 |
Data reduction software | DENZO |
Data scaling software | SCALA (3.3.22) |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 62.345 | 62.345 | 2.030 |
High resolution limit [Å] | 1.929 | 6.100 | 1.930 |
Rmerge | 0.109 | 0.034 | 0.645 |
Rmeas | 0.135 | 0.041 | 0.777 |
Rpim | 0.060 | 0.019 | 0.348 |
Number of reflections | 28742 | 1019 | 4165 |
<I/σ(I)> | 9.5 | 13.7 | 1.1 |
Completeness [%] | 99.8 | 99.6 | 99.9 |
Redundancy | 4.8 | 4.5 | 4.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 310 | orthorhombic shaped crystals |