6EDC
hcGAS-16bp dsDNA complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-07-02 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9792 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 99.813, 99.813, 238.644 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 86.441 - 2.712 |
R-factor | 0.2409 |
Rwork | 0.239 |
R-free | 0.27760 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4k96 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.509 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 86.441 | 2.800 |
High resolution limit [Å] | 2.710 | 2.710 |
Number of reflections | 19571 | |
<I/σ(I)> | 11.3 | |
Completeness [%] | 99.1 | 96.1 |
Redundancy | 12 | |
CC(1/2) | 0.996 | 0.506 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.2 M NaCl, 0.1 M HEPES, pH 7.5, and 28% PEG400 (v/v) |