6E8J
Crystal Structure of A Bacterial Homolog to Human Lysosomal Transporter, Spinster, in Inward-facing And Occupied Conformation
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 93 |
Detector technology | PIXEL |
Collection date | 2017-08-08 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.977760 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 88.709, 89.419, 122.140 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.710 - 3.091 |
R-factor | 0.2612 |
Rwork | 0.257 |
R-free | 0.29760 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.138 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.280 |
High resolution limit [Å] | 3.090 | 3.090 |
Rmerge | 0.109 | |
Number of reflections | 18325 | |
<I/σ(I)> | 17.5 | |
Completeness [%] | 99.7 | |
Redundancy | 13.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.4 | 277 | 32.5%(v/v) PEG 400, 100 mM Tris-HCl |