6E8H
Legionella Longbeachae LeSH (Llo2327)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 114 |
Detector technology | IMAGE PLATE |
Collection date | 2012-12-01 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.54 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 42.260, 66.510, 68.210 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.630 - 1.680 |
R-factor | 0.2137 |
Rwork | 0.212 |
R-free | 0.24750 |
Structure solution method | SAD |
RMSD bond length | 0.006 |
RMSD bond angle | 0.800 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | Auto-Rickshaw |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.630 | 1.760 |
High resolution limit [Å] | 1.660 | 1.660 |
Rmerge | 0.052 | 0.284 |
Number of reflections | 22693 | 2832 |
<I/σ(I)> | 68.2 | 16.9 |
Completeness [%] | 97.5 | 85 |
Redundancy | 55.7 | 50.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 278 | Tris, PEG3000, sodium acetate |