6E6A
Triclinic crystal form of IncA G144A point mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-09-21 |
Detector | DECTRIS PILATUS3 R 200K-A |
Wavelength(s) | 1.54 |
Spacegroup name | P 1 |
Unit cell lengths | 41.022, 43.533, 45.783 |
Unit cell angles | 92.93, 95.96, 93.91 |
Refinement procedure
Resolution | 14.960 - 1.950 |
R-factor | 0.172 |
Rwork | 0.170 |
R-free | 0.21300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6e7e |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | AutoSol |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.000 | 2.020 |
High resolution limit [Å] | 1.950 | 1.950 |
Number of reflections | 20042 | 1478 |
<I/σ(I)> | 20.4 | 5.8 |
Completeness [%] | 88.1 | 66.3 |
Redundancy | 1.5 | 1.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 295 | 0.2 M sodium acetate trihydrate, pH 8.0, 20% w/v PEG3350 |