6E60
Bacteroides ovatus mixed-linkage glucan utilization locus (MLGUL) SGBP-A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-11-24 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 47.279, 89.367, 120.941 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.250 - 1.500 |
R-factor | 0.1591 |
Rwork | 0.158 |
R-free | 0.18400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | unpublished |
RMSD bond length | 0.012 |
RMSD bond angle | 1.582 |
Data reduction software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0230) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.590 |
High resolution limit [Å] | 1.500 | 1.500 |
Number of reflections | 81232 | 12744 |
<I/σ(I)> | 9.84 | 1.49 |
Completeness [%] | 97.6 | 95.9 |
Redundancy | 4.48 | 4.49 |
CC(1/2) | 0.997 | 0.605 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 296 | 0.2M magnesium chloride, 0.1M bis-tris, 25% (w/v) PEG3350 |