6E33
Crystal Structure of Pho7-DNA complex
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-06-21 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.2827, 0.97918 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 50.827, 40.682, 58.237 |
Unit cell angles | 90.00, 105.84, 90.00 |
Refinement procedure
Resolution | 43.131 - 1.705 |
R-factor | 0.1893 |
Rwork | 0.188 |
R-free | 0.21520 |
Structure solution method | SAD |
RMSD bond length | 0.006 |
RMSD bond angle | 0.886 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SHELXCD |
Refinement software | PHENIX ((1.12_2829)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.750 |
High resolution limit [Å] | 1.700 | 1.700 |
Rpim | 0.040 | |
Number of reflections | 24169 | 1086 |
<I/σ(I)> | 24.1 | 2.5 |
Completeness [%] | 96.1 | 87.4 |
Redundancy | 5.5 | 3.6 |
CC(1/2) | 0.932 | 0.953 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | Tris-HCl pH 7.0, 0.2M NaOAc, 32.5% PEG 4000 |