6DYS
C-terminal condensation domain of Ebony in complex with beta-alanyl-dopamine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-10-13 |
Detector | ADSC QUANTUM 210r |
Wavelength(s) | 0.9537 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 44.481, 56.494, 49.934 |
Unit cell angles | 90.00, 113.50, 90.00 |
Refinement procedure
Resolution | 45.790 - 2.300 |
R-factor | 0.174 |
Rwork | 0.172 |
R-free | 0.20490 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6dym |
RMSD bond length | 0.004 |
RMSD bond angle | 0.647 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX (1.13_2998) |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.790 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Number of reflections | 10138 | |
<I/σ(I)> | 14.2 | |
Completeness [%] | 99.4 | |
Redundancy | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 293 | HEPES, PEG400, CaCl2 |