6DVS

Crystal structure of Pseudomonas stutzeri D-phenylglycine aminotransferase

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	100
Detector technology	PIXEL
Collection date	2014-03-21
Detector	DECTRIS PILATUS 6M
Wavelength(s)	1.0000
Spacegroup name	P 31 2 1
Unit cell lengths	74.639, 74.639, 149.948
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	49.983 - 1.821
R-factor	0.181
Rwork	0.179
R-free	0.22230
RMSD bond length	0.006
RMSD bond angle	0.750
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX ((1.13_2998: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	49.983	2.040
High resolution limit [Å]	1.820	1.820
Number of reflections	44043
<I/σ(I)>	78.4
Completeness [%]	99.8
Redundancy	8.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		290	1 M ammonium sulfate