6DTR
Apo T. maritima MalE3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2018-06-01 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 65.500, 137.478, 145.019 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.541 - 2.301 |
R-factor | 0.1653 |
Rwork | 0.164 |
R-free | 0.19310 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1eu8 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.734 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.129 | 0.641 |
Number of reflections | 27256 | 2661 |
<I/σ(I)> | 2 | |
Completeness [%] | 92.5 | |
Redundancy | 2.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 20% PEG 4000 and 0.2M sodium sulfate |