Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE F1 |
| Synchrotron site | CHESS |
| Beamline | F1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-11-19 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9782 |
| Spacegroup name | I 4 |
| Unit cell lengths | 175.049, 175.049, 76.598 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 29.923 - 2.694 |
| R-factor | 0.193 |
| Rwork | 0.191 |
| R-free | 0.22260 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.375 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 29.923 | 2.761 |
| High resolution limit [Å] | 2.694 | 2.694 |
| Number of reflections | 31537 | |
| <I/σ(I)> | 32.6 | |
| Completeness [%] | 97.9 | |
| Redundancy | 4.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 300 | 0.17 M sodium acetate, 0.085 M sodium cacodylate (pH 6.5), 15% PEG8000, 15% glycerol and 5 microM spermine |
