Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE F1 |
| Synchrotron site | CHESS |
| Beamline | F1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-11-19 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9782 |
| Spacegroup name | I 4 |
| Unit cell lengths | 174.760, 174.760, 76.404 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 41.191 - 3.200 |
| R-factor | 0.1952 |
| Rwork | 0.190 |
| R-free | 0.24280 |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.386 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 41.191 | 3.280 |
| High resolution limit [Å] | 3.200 | 3.200 |
| Number of reflections | 19223 | |
| <I/σ(I)> | 13.7 | |
| Completeness [%] | 99.9 | |
| Redundancy | 4.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 300 | 0.17 M sodium acetate, 0.085 M sodium cacodylate (pH 6.5), 15% PEG8000, 15% glycerol and 5 microM spermine |
