6DSW
Bst DNA polymerase I pre-chemistry (n) structure
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.2 |
Synchrotron site | ALS |
Beamline | 8.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-10-24 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 86.139, 93.410, 105.619 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 63.324 - 1.589 |
R-factor | 0.166 |
Rwork | 0.166 |
R-free | 0.18970 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1l3s |
RMSD bond length | 0.006 |
RMSD bond angle | 0.821 |
Data reduction software | autoXDS |
Data scaling software | autoXDS |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 64.000 | 1.646 |
High resolution limit [Å] | 1.589 | 1.589 |
Rmerge | 0.730 | 1.350 |
Number of reflections | 115054 | 11362 |
<I/σ(I)> | 71.43 | |
Completeness [%] | 100.0 | |
Redundancy | 31.3 | |
CC(1/2) | 0.827 | 0.794 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 50% ammonium sulfate, 0.1M MES, 2% MPD |