6DNQ
HBZ77 in complex with KIX and c-Myb
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-11-16 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 118.825, 51.166, 72.047 |
Unit cell angles | 90.00, 126.41, 90.00 |
Refinement procedure
Resolution | 36.019 - 2.350 |
R-factor | 0.2001 |
Rwork | 0.199 |
R-free | 0.22890 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2agh |
RMSD bond length | 0.004 |
RMSD bond angle | 0.721 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10_2155)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.390 |
High resolution limit [Å] | 2.350 | 2.350 |
Rmerge | 0.120 | |
Rmeas | 0.130 | |
Rpim | 0.060 | |
Number of reflections | 14320 | |
<I/σ(I)> | 13.7 | |
Completeness [%] | 97.1 | |
Redundancy | 4.5 | |
CC(1/2) | 0.870 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | PEG 3350, calcium chloride |