6DNM
The crystal structure of SatS c-terminal domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 120 |
Detector technology | PIXEL |
Collection date | 2018-04-14 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.979 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 48.867, 50.580, 76.465 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.186 - 1.397 |
R-factor | 0.1947 |
Rwork | 0.193 |
R-free | 0.23070 |
RMSD bond length | 0.005 |
RMSD bond angle | 0.736 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 99.000 | 1.420 |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.081 | 0.254 |
Number of reflections | 35457 | |
<I/σ(I)> | 14.4 | |
Completeness [%] | 92.6 | |
Redundancy | 5.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289 | 3.5M ammonium citrate |