6DLF
Crystal structure of NTRI homodimer
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE F1 |
Synchrotron site | CHESS |
Beamline | F1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-06-26 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.98 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 76.517, 101.996, 134.025 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.664 - 3.446 |
R-factor | 0.275 |
Rwork | 0.274 |
R-free | 0.30450 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6dld |
RMSD bond length | 0.003 |
RMSD bond angle | 0.758 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.664 | 3.650 |
High resolution limit [Å] | 3.446 | 3.450 |
Number of reflections | 14368 | |
<I/σ(I)> | 10.7 | |
Completeness [%] | 99.7 | |
Redundancy | 6.3 | |
CC(1/2) | 0.998 | 0.758 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | Na,K-Tartrate, Tris-HCl pH 8.5 |