6DKA
Yeast Ddi2 Cyanamide Hydratase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08B1-1 |
Synchrotron site | CLSI |
Beamline | 08B1-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-02-20 |
Detector | RAYONIX MX300HE |
Wavelength(s) | 1.0246 |
Spacegroup name | P 3 2 1 |
Unit cell lengths | 263.430, 263.430, 119.214 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.966 - 2.901 |
R-factor | 0.1986 |
Rwork | 0.198 |
R-free | 0.22960 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 6dk9 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.845 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.13_2998)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.300 | 2.950 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.114 | 0.630 |
Number of reflections | 101420 | 5107 |
<I/σ(I)> | 16.1 | 2.2 |
Completeness [%] | 96.8 | 98.4 |
Redundancy | 6.6 | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.8 | 298 | 1.1-1.3 M Ammonium Sulfate 0.2 M Arginine 0.1 M N-morpholino ethane sulfonate pH 5.8 |