6DK8
RetS kinase region without cobalt
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 31-ID |
Synchrotron site | APS |
Beamline | 31-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-07-21 |
Detector | RAYONIX MX225HE |
Wavelength(s) | 0.9739 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 158.708, 158.708, 243.826 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 56.779 - 3.800 |
R-factor | 0.2155 |
Rwork | 0.215 |
R-free | 0.24870 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6dk7 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.754 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHENIX |
Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 56.780 | 3.936 |
High resolution limit [Å] | 3.800 | 3.800 |
Number of reflections | 31211 | |
<I/σ(I)> | 8.1 | |
Completeness [%] | 100.0 | |
Redundancy | 26.2 | |
CC(1/2) | 0.999 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 277 | 2.7 M sodium chloride, 0.1 M HEPES, pH 7.5 |