6DK4
Crystal structure of Campylobacter jejuni peroxide stress regulator
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-01-25 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.2822 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 48.110, 70.186, 85.158 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 54.000 - 2.710 |
R-factor | 0.2176 |
Rwork | 0.215 |
R-free | 0.27010 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.210 |
Data reduction software | XDS |
Data scaling software | autoPROC |
Phasing software | AutoSol |
Refinement software | BUSTER (2.10.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 54.000 | 2.720 |
High resolution limit [Å] | 2.710 | 2.710 |
Number of reflections | 8254 | |
<I/σ(I)> | 24 | |
Completeness [%] | 100.0 | |
Redundancy | 14.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277.15 | 0.1 M HEPES, pH 7.2-7.4, 35-60% MPD |