6DHS
Structure of hnRNP H qRRM1,2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-F |
Synchrotron site | APS |
Beamline | 21-ID-F |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-07-08 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 0.9787 |
Spacegroup name | P 64 2 2 |
Unit cell lengths | 204.670, 204.670, 123.790 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 45.690 - 3.500 |
R-factor | 0.306 |
Rwork | 0.306 |
R-free | 0.32200 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.000 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 3.560 |
High resolution limit [Å] | 3.500 | 9.480 | 3.500 |
Rmerge | 0.148 | 0.067 | 0.835 |
Rmeas | 0.150 | 0.069 | 0.848 |
Rpim | 0.027 | 0.013 | 0.150 |
Total number of observations | 606047 | ||
Number of reflections | 21278 | 1104 | 953 |
<I/σ(I)> | 5.7 | ||
Completeness [%] | 100.0 | 99.7 | 100 |
Redundancy | 30.9 | 26.5 | 31.3 |
CC(1/2) | 0.997 | 0.999 | 0.945 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | 30-50% peg 400 and 0.1M phosphate-citrate, pH 4.2 |