6DFV
Mouse diabetogenic TCR 8F10
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-12-13 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.979500 |
Spacegroup name | P 1 |
Unit cell lengths | 62.016, 69.691, 69.699 |
Unit cell angles | 111.66, 111.03, 94.86 |
Refinement procedure
Resolution | 48.210 - 1.710 |
R-factor | 0.17389 |
Rwork | 0.171 |
R-free | 0.23113 |
RMSD bond length | 0.015 |
RMSD bond angle | 1.715 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0222) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.800 |
High resolution limit [Å] | 1.710 | 1.710 |
Number of reflections | 91564 | |
<I/σ(I)> | 11.62 | |
Completeness [%] | 91.5 | |
Redundancy | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 14% PEG 3350, 100mM sodium acetate at pH6.0 |