6DBE
Crystal Structure of VHH R330
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-12-12 |
Detector | RAYONIX MX-300 |
Wavelength(s) | 0.97950 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 58.615, 58.615, 100.527 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 45.313 - 1.650 |
R-factor | 0.1868 |
Rwork | 0.185 |
R-free | 0.22270 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6dba |
RMSD bond length | 0.010 |
RMSD bond angle | 1.152 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.760 | 50.760 | 1.690 |
High resolution limit [Å] | 1.650 | 7.380 | 1.650 |
Rmerge | 0.100 | 0.050 | 0.497 |
Number of reflections | 24176 | ||
<I/σ(I)> | 9.5 | 11.4 | 3.8 |
Completeness [%] | 98.4 | 73.9 | 95.1 |
Redundancy | 4.5 | 3.2 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | 0.1M HEPES, 25% PEG 3350 |