6D8L
Group I self-splicing intron P4-P6 domain mutant U131A (without isopropanol soaking)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-12-08 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.979100 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 75.480, 132.950, 147.540 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 67.197 - 3.140 |
R-factor | 0.251022611814 |
Rwork | 0.250 |
R-free | 0.26960 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1gid |
RMSD bond length | 0.003 |
RMSD bond angle | 0.732 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 67.200 | 3.220 |
High resolution limit [Å] | 3.140 | 3.140 |
Number of reflections | 25498 | |
<I/σ(I)> | 12.9 | |
Completeness [%] | 95.9 | |
Redundancy | 10.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | MPD, sodium cacodylate, cobalt hexamine |