6D7C
The crystal structure of hemagglutinin from A/Hong Kong/61/2016 H7N9 influenza virus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-BM |
Synchrotron site | APS |
Beamline | 22-BM |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-08-07 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 1.0 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 210.014, 97.527, 191.809 |
Unit cell angles | 90.00, 108.58, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.950 |
R-factor | 0.23783 |
Rwork | 0.236 |
R-free | 0.26703 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ln6 |
RMSD bond length | 0.015 |
RMSD bond angle | 1.896 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.060 |
High resolution limit [Å] | 2.950 | 2.950 |
Number of reflections | 68692 | |
<I/σ(I)> | 6.43 | |
Completeness [%] | 93.1 | |
Redundancy | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICROBATCH | 293 | 0.2 M Magnesium Chloride, 0.1M HEPES:NaOH, pH7.5, 25% PEG 3350 |