6D6G
Triclinic lysozyme (295 K) in the presence of 47% MPD
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | Agilent SuperNova |
Temperature [K] | 295 |
Detector technology | CCD |
Collection date | 2016-01-20 |
Detector | OXFORD ONYX CCD |
Wavelength(s) | 1.54 |
Spacegroup name | P 1 |
Unit cell lengths | 27.333, 32.151, 34.318 |
Unit cell angles | 88.24, 70.78, 68.69 |
Refinement procedure
Resolution | 13.613 - 2.000 |
R-factor | 0.1337 |
Rwork | 0.132 |
R-free | 0.18190 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.501 |
Data scaling software | SCALA |
Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 13.620 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmeas | 0.072 | 0.278 |
Number of reflections | 6714 | |
<I/σ(I)> | 13.1 | 4.4 |
Completeness [%] | 97.3 | |
Redundancy | 2.3 | |
CC(1/2) | 0.997 | 0.909 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 295 | Protein: 10 mg/mL in water Well: 0.3 M NaNO3 |