6D69
Crystal Structure of the NHL Repeat Region of D. melanogaster Thin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-BM |
Synchrotron site | APS |
Beamline | 22-BM |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-12-09 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 1.00 |
Spacegroup name | P 65 |
Unit cell lengths | 132.727, 132.727, 49.704 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 43.445 - 2.601 |
R-factor | 0.1894 |
Rwork | 0.186 |
R-free | 0.21940 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1q7f |
RMSD bond length | 0.014 |
RMSD bond angle | 1.502 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.690 |
High resolution limit [Å] | 2.600 | 5.600 | 2.600 |
Rmerge | 0.128 | 0.052 | 0.680 |
Number of reflections | 15485 | 1633 | 1404 |
<I/σ(I)> | 14.36 | ||
Completeness [%] | 99.0 | 99.5 | 91.9 |
Redundancy | 7.2 | 7.7 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.8 | 293 | 0.1 M HEPES (pH 7.8) 0.2 M sodium chloride 25% (w/v) peg-3350 |