6D57
Campylobacter jejuni ferric uptake regulator S1 metalated
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-ID |
| Synchrotron site | APS |
| Beamline | 17-ID |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-02-08 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 35.742, 84.363, 123.626 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 69.680 - 1.810 |
| R-factor | 0.186 |
| Rwork | 0.184 |
| R-free | 0.22900 |
| RMSD bond length | 0.016 |
| RMSD bond angle | 1.300 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.10.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 69.680 | 1.900 |
| High resolution limit [Å] | 1.810 | 1.810 |
| Number of reflections | 34641 | |
| <I/σ(I)> | 5.3 | |
| Completeness [%] | 100.0 | |
| Redundancy | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 277 | 0.1 M Bis-Tris, pH 5.5, 0.25 M magnesium formate, 25% PEG3350 |
