6D0J
Crystal structure of a CLC-type fluoride/proton antiporter
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.1 |
Synchrotron site | ALS |
Beamline | 5.0.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-04-30 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97741 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 116.972, 126.421, 133.947 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.350 - 3.000 |
R-factor | 0.2405 |
Rwork | 0.239 |
R-free | 0.26030 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3q17 5FXB |
RMSD bond length | 0.002 |
RMSD bond angle | 0.465 |
Data reduction software | xia2 |
Data scaling software | DIALS |
Phasing software | PHASER |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.350 | 3.120 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.073 | 3.520 |
Number of reflections | 40496 | 4523 |
<I/σ(I)> | 19.4 | 1.3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 34.5 | 32.8 |
CC(1/2) | 1.000 | 0.825 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 295 | 10 mM HEPES, pH 7.0 100 mM ADA, pH 6.0 100 mM NaF 100 mM K Formate 20% PEG 600 |