6D0H
ParT: Prs ADP-ribosylating toxin bound to cognate antitoxin ParS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-12-08 |
Detector | DECTRIS PILATUS3 R 300K |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 |
Unit cell lengths | 41.867, 51.342, 57.797 |
Unit cell angles | 84.31, 73.93, 84.78 |
Refinement procedure
Resolution | 24.625 - 1.500 |
R-factor | 0.149 |
Rwork | 0.148 |
R-free | 0.17500 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.100 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MERLOT |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 40.000 | 40.000 | 1.480 |
High resolution limit [Å] | 1.450 | 3.930 | 1.450 |
Rmerge | 0.048 | 0.032 | 0.202 |
Rmeas | 0.057 | 0.038 | 0.282 |
Rpim | 0.029 | 0.019 | 0.196 |
Total number of observations | 220685 | ||
Number of reflections | 76745 | 4052 | 1965 |
<I/σ(I)> | 19.3 | ||
Completeness [%] | 94.1 | 99.6 | 48.1 |
Redundancy | 2.9 | 3.7 | 1.2 |
CC(1/2) | 0.998 | 0.878 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 293 | 10% MPD, 100 mM sodium acetate trihydrate |