6CZU
BRD4(BD1) complexed with 3219
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X29A |
Synchrotron site | NSLS |
Beamline | X29A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-11-25 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.075 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 43.066, 48.967, 59.880 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.340 - 1.470 |
R-factor | 0.1474 |
Rwork | 0.145 |
R-free | 0.19420 |
RMSD bond length | 0.023 |
RMSD bond angle | 2.246 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.520 |
High resolution limit [Å] | 1.470 | 3.170 | 1.470 |
Rmerge | 0.129 | 0.109 | 0.483 |
Total number of observations | 148794 | ||
Number of reflections | 22125 | 2362 | 2168 |
<I/σ(I)> | 17 | ||
Completeness [%] | 99.9 | 99 | 100 |
Redundancy | 6.7 | 6.5 | 6.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 297 | 0.2 M Ammonium Sulfate, 0.1 M Bis-Tris pH 6.5, 25% PEG 3350 |