6CR9
Ternary complex crystal structure of DNA polymerase Beta with a dideoxy terminated primer with CFCL, beta, gamma dATP analogue
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-03-14 |
Detector | RIGAKU SATURN 944 |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 50.748, 79.466, 55.651 |
Unit cell angles | 90.00, 107.61, 90.00 |
Refinement procedure
Resolution | 23.892 - 1.960 |
R-factor | 0.1825 |
Rwork | 0.180 |
R-free | 0.22370 |
RMSD bond length | 0.007 |
RMSD bond angle | 0.972 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.990 |
High resolution limit [Å] | 1.960 | 5.320 | 1.960 |
Rmerge | 0.080 | 0.059 | 0.430 |
Total number of observations | 107698 | ||
Number of reflections | 30271 | 1555 | 1423 |
<I/σ(I)> | 8.6 | ||
Completeness [%] | 99.5 | 98.7 | 94.1 |
Redundancy | 3.6 | 3.6 | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 16-18% PEG 3350 |