6CLX
Crystal structure of TnmH in complex with SAM
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2017-12-10 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.5418 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 116.220, 116.220, 110.400 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 55.240 - 2.730 |
R-factor | 0.22793 |
Rwork | 0.225 |
R-free | 0.27780 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6clw |
RMSD bond length | 0.008 |
RMSD bond angle | 1.354 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 55.240 | 2.880 |
High resolution limit [Å] | 2.730 | 2.730 |
Rmerge | 0.148 | 0.871 |
Rpim | 0.088 | 0.554 |
Number of reflections | 23384 | 3362 |
<I/σ(I)> | 10.4 | |
Completeness [%] | 100.0 | |
Redundancy | 7 | |
CC(1/2) | 0.995 | 0.580 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 0.2 M L-Proline, 0.1 M HEPES, pH 7.5, 10% w/v Polyethlene glycol 3,350 |