6CJL
Candida albicans Hsp90 nucleotide binding domain in complex with radicicol
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 120 |
Detector technology | CCD |
Collection date | 2015-08-25 |
Detector | RAYONIX MX-300 |
Wavelength(s) | 0.97949 |
Spacegroup name | P 43 |
Unit cell lengths | 73.100, 73.100, 109.514 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.597 - 1.697 |
Rwork | 0.145 |
R-free | 0.16530 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.760 |
High resolution limit [Å] | 1.670 | 1.670 |
Rmerge | 0.100 | 0.500 |
Number of reflections | 66682 | 9675 |
<I/σ(I)> | 14.6 | 4.7 |
Completeness [%] | 99.9 | 99.8 |
Redundancy | 9.9 | 9.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 298.15 | 8% Tacsimate 20% PEG3350 |