6CIU
Structure of a Thr-rich interface in an Azami Green tetramer
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-12-09 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9793 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 70.505, 86.184, 141.750 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 73.640 - 1.700 |
R-factor | 0.16656 |
Rwork | 0.165 |
R-free | 0.20509 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3adf |
RMSD bond length | 0.027 |
RMSD bond angle | 2.469 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 73.640 | 1.730 |
High resolution limit [Å] | 1.700 | 1.700 |
Number of reflections | 91590 | |
<I/σ(I)> | 16 | |
Completeness [%] | 97.1 | |
Redundancy | 2.6 | |
CC(1/2) | 0.998 | 0.780 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | 0.1 M Magnesium chloride hexahydrate, 100 mM Tris pH 8.5, 25% w/v PEG 3350 |