6CFY
Bosea sp Root 381 apo GapR structure
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 273 |
Detector technology | PIXEL |
Collection date | 2017-12-16 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 41 2 2 |
Unit cell lengths | 39.589, 39.589, 205.125 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.800 - 2.400 |
R-factor | 0.2344 |
Rwork | 0.231 |
R-free | 0.26590 |
Structure solution method | SAD |
RMSD bond length | 0.018 |
RMSD bond angle | 1.675 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AutoSol |
Refinement software | PHENIX (1.6.4_486) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.870 | 2.530 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmeas | 0.122 | |
Rpim | 0.041 | |
Number of reflections | 12187 | 1213 |
<I/σ(I)> | 11.2 | |
Completeness [%] | 100.0 | 99.9 |
Redundancy | 19.1 | |
CC(1/2) | 0.997 | 0.319 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 15% MPD, 10 mM MgCl2, HEPES (7.5) 0.001 M spermine |